GC/MS Monitoring of Selected PAHs in Soil Samples Using Ultrasound-assisted QuEChERS in Tandem with Dispersive Liquid-Liquid Microextraction
نویسندگان
چکیده
منابع مشابه
Dispersive liquid-liquid microextraction coupled with magnetic nanoparticles for extraction of zearalenone in wheat samples
A new, sensitive and fast dispersive liquid-liquid microextraction (DLLME) coupled with micro-solid phase extraction (μ-SPE) was developed for determination of zearalenone (ZEN) in wheat samples. The DLLME was performed using acetonitrile/water (80:20 v/v) as the disperser solvent and 1-octanol as the extracting solvent. The acetonitrile/water (80:20 v/v) solvent was also used to extract ZEN f...
متن کاملSpectrophotometric determination of iron species using ionic liquid ultrasound assisted dispersive liquid–liquid microextraction
A simple and efficient method for speciation and determination of iron in different water samples was developed. The method is based on ionic liquid ultrasound assisted dispersive liquid–liquid microextraction (IL-USADLLME) followed by spectrophotometric determination. Fe(II) is complexed with 2,4,6-tri(2’-pyridyl)-l,3,5-triazine (TPTZ), neutralized through ion pair formation with sodium dodecy...
متن کاملSpectrophotometric Determination of Formaldehyde in Seawater Samples after In-situ Derivatization and Dispersive Liquid-Liquid Microextraction
In this paper, a simple dispersive liquid-liquid microextraction for the extraction and pre-concentration of formaldehyde in seawater samples followed with spectrophotometric is proposed. Formaldehyde was derivatized in situ with acetyl acetone in the presence of ammonium acetate in a single step. Then it was collected into a mixture of ethanol (disperser solvent) and chloroform (extracting...
متن کاملApplication of Dispersive Liquid-Liquid Microextraction to Determine Aflatoxin B1 in Tomato Paste Samples
Background: Aflatoxin B1 is a secondary toxic metabolite produced by several aspergillus species. This study was conducted to determine the presence of aflatoxin in tomato paste samples. Methods: A total of 30 tomato pastes were analyzed for Aflatoxin B1 contamination via HPLC-FLD. Analyte extraction was done by dispersive liquid-liquid microextraction. Results: The limit of detection (LOD) and...
متن کاملDetermination of Pyrethroid Pesticides in Environmental Samples using Ionic Liquid Dispersive Liquid-Liquid Microextraction
Microextração líquido-líquido dispersiva (DLLME) utilizando líquido iônico (IL) como solvente extrator foi desenvolvida com uma nova abordagem para a determinação de quatro pesticidas piretróides em amostras ambientais de água e solo. Cromatografia líquida de alto rendimento com detector de UV (HPLC-UV) foi empregada na análise cromatográfica. Este método é rápido, fácil de operar e ambientalme...
متن کاملذخیره در منابع من
با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید
ژورنال
عنوان ژورنال: International Journal of Environmental Monitoring and Analysis
سال: 2015
ISSN: 2328-7659
DOI: 10.11648/j.ijema.20150305.17